1.TURN ON THE JACKET CIRCULATING PUMP, AND TURN ON THE HOT WATER HEATER. 1、打开夹套循环泵，再打开热水加热器。2. TURN OFF THE HOT WATER HEATER WHEN THE JACKET INLET TEMPERATURE REACHES 28oC. 2、当夹套入口水温达到28度时，关闭热水加热器。 3.WHEN THE REACTOR VESSEL TEMPERATURE APPROACHES 27oC, TURN OFF THE JACKET PUMP, OPEN THE JACKET BYPASS VALVE, AND CLOSE THE INLET AND OUTLET VALVES. 3、当反应釜温度接近27度时，关闭夹套循环泵，打开夹套的旁通阀，并关闭夹套入口和出口的阀门4. WHEN THE REACTOR VESSEL TEMPERATURE REACHES 27oC TO 28oC, OPEN THE CITY WATER VALVE AND THE JACKET DRAIN VALVE AND ADJUST THE JACKET INLET AND OUTLET TEMPERATURES AS CLOSE AS POSSIBLE TO 27oC. THE INLET TEMPERATURE MAY BE SLIGHTLY LOWER TO GET THE OUTLET TEMPERATURE WITHIN RANGE. 4、当反应釜温度达到27~28度，同时打开自来水阀门和夹套进出口阀门，将夹套温度尽可能调节到27度。夹套入口的温度可能会稍微低于夹套出口的温度，伴有波动。1 HEAT THE FLASK TO REFLUX AND REMOVE WATER WITH A BARRETT TRAP. 1、将烧瓶加热至回流，并用一个疏水阀将水分离出来2 REMOVE 138 mls OF SOLVENT FROM BARRETT TRAP. . 2 从疏水阀中分离出138毫升溶液3 COOL THE FLASK TO 75 DEG C. 3 将烧瓶冷却至75摄氏度4 AFTER THE WATER HAS BEEN REMOVED, REDUCE AGITATOR SPEED TO 300-325 RPM.4 当水移除之后，降低搅拌速度至300-325转/分钟5. DRAIN ANY REMAINING LIQUID IN BARRETT TRAP TO COLLECTION FLASK. 5 从疏水阀中移除所有的液体到收集烧瓶6 REMOVE CONDENSER, RINSE WITH THF AND BLOW DRY WITH AIR. 6 清洗冷凝器，用THF清洗，并用压缩空气吹干7 REMOVE BARRETT TRAP AND REPLACE IT WITH CONDSENER. 7 用冷凝气替代疏水阀8. RINSE BARRETT TRAP WITH THF. BLOW DRY WITH AIR. RETURN IT TO STORAGE RACK.8 用THF冲洗疏水阀，并用压缩空气吹干，重新放回货架你这个是传统的反应釜控温步骤吧，操作有些繁琐的。夹套反应釜用水进行控温的话，下次建议你直接买个夹套式反应釜（釜本身不带电加热功能），然后配一台循环水加热器，可以自动控温的，最普通的机型出水温度也能控制到正负1度。
零碎的回忆123
